Influence of the crystallization kinetics on the microstructural properties of γ-PVDF

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dc.contributor.authorSilva, M. P.
dc.contributor.authorSencadas, Vítor João Gomes Silva
dc.contributor.authorRolo, Anabela G.
dc.contributor.authorBotelho, Gabriela
dc.contributor.authorMachado, A. V.
dc.contributor.authorRocha, J. G.
dc.contributor.authorLanceros-Méndez, S.
dc.date.accessioned2012-04-26T11:04:01Z
dc.date.available2012-04-26T11:04:01Z
dc.date.issued2008
dc.description.abstractThe kinetics of the isothermal crystallization of the γ-phase Poly(vinylidene fluoride) has been investigated. Samples were prepared from the melt at different crystallisation temperatures and the variation of the microstructure of the samples was monitored with time by optical microscopy. Raman and Infrared transmission spectroscopies also show the appearance of the γ-phase for higher crystallisation temperatures. Two types of γ-phase spherulites have been identified. These spherulites represents different ways to obtain the γ-phase and show different thermal stability. The correlation between microstructure and kinetic parameters allows the tailoring of the microstructure by choosing the crystallisation conditions of the samples.por
dc.description.sponsorshipThe authors thank the Portuguese Foundation for Science and Technology (FCT) for financial support (Grant POCI/CTM/59425/2004). V. Sencadas also thanks the FCT for the PhD Grant (SFRH/BD/16543/2004). The authors also thank to Solvay for providing the excellent quality material.por
dc.distributioninternational
dc.identifier.citationSilva, M. P., Sencadas, V., Rolo, A. G., Botelho, G., Machado, A. V., Rocha, J. G., & Lanceros-Méndez, S. (2008, June). Influence of the Crystallization Kinetics on the Microstructural Properties of γ-PVDF. Materials Science Forum. Trans Tech Publications, Ltd. http://doi.org/10.4028/www.scientific.net/msf.587-588.534
dc.identifier.doi10.4028/www.scientific.net/MSF.587-588.534
dc.identifier.issn0255-5476por
dc.identifier.urihttps://hdl.handle.net/1822/18893
dc.language.isoengpor
dc.peerreviewedyespor
dc.publisherTrans Tech Publicationspor
dc.relationinfo:eu-repo/grantAgreement/FCT/POCI/POCI%2FCTM%2F59425%2F2004/PT
dc.relationinfo:eu-repo/grantAgreement/FCT/PIDDAC/SFRH%2FBD%2F16543%2F2004/PT
dc.rightsrestrictedAccesspor
dc.subjectPVDFpor
dc.subjectCrystallizationpor
dc.subjectDSCpor
dc.subjectInfrared spectroscopypor
dc.subjectRaman spectroscopypor
dc.subject.wosScience & Technologypor
dc.titleInfluence of the crystallization kinetics on the microstructural properties of γ-PVDFpor
dc.typeconferencePaper
dspace.entity.typePublicationen
oaire.citationEndPage537por
oaire.citationStartPage534por
oaire.citationTitleMaterials Science Forumpor
oaire.citationVolume587-588por
sdum.conferencePublicationADVANCED MATERIALS FORUM IVpor
sdum.journalMaterials Science Forumpor
sdum.publicationstatuspublishedpor

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Influence of the Crystallization Kinetics on the Microstructural Properties of γ-PVDF
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